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Performance Optimization of Electrochemical Sensor based on Iron Oxide-reduced Graphene Oxide Nanocomposite: Application for Environmental Monitoring

Amira Ghezal, Ammar Al-Hamry, Leonardo G. Paterno, Mounir Ben Ali, Olfa Kanoun

Abstract

In this work, an electrochemical sensor based on iron oxide-reduced graphene oxide nanococmposite modified screen printed graphite electrode (Fe<sub>3</sub>O<sub>4</sub>-rGO/SPGE) has been developed for selective detection of nitrite ions in drinking water using differential pulse voltammetry (DPV). The proposed nitrite electrochemical sensor exhibited a relative standard deviation of 4.37% for three replicate analysis of 10<sup>-3</sup> M L<sup>-1</sup> NO<sub>2</sub>. In addition, it displays high electrochemical stability for nitrite oxidation over the pH 6.5, high sensitivity and low limit of detection of 1.2 x 10<sup>-5</sup> M L<sup>-1</sup> with good selectivity in the concentration range 10<sup>-4</sup> - 10<sup>-3</sup> which is the range where the rate of nitrite is maximum. These results prove that the metal oxide-rGO nanocomposite modified SPGE has good applications for the determination of nitrite in water.

Keywords
Iron Oxide-reduced graphene oxide nanocomposites, Electrochemical detection, Nitrite sensor
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IMEKO-TC19-2019-02.pdf
DOI
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IMEKO TC
TC19 - Environmental Measurements

Event details

Event
tc19-2019

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