INDENTATION VELOCITY EFFECT ON MARTENS HARDNESS MEASUREMENT

K. Herrmann, A. Germak, F. Menelao, G. Barbato, G. Brondino
Abstract:
The Martens Hardness (HM) is an important parameter characterising the elasticplastic properties of the to be investigated sample material which is derived from the instrumented indentation test. At present the standardisation of the instrumented indentation test in the framework of ISO/DIS 14577-1, -2, -3 is underway. This standard addresses the macro-, micro- and nanorange of the indentation test. The peculiarities of the nanoindentation test when measuring samples with thin coatings (coating thickness d < 2 µm) will be considered in ISO/CD 14577-4 for which inputs came from CEN TC 184/WG 5 and from the EU-project „INDICOAT“. Martens Hardness presents a number of advantages, but, as any newly defined method, requires a general analysis of influence quantities to determine the sensitivity coefficients necessary for the uncertainty evaluation. Indentation velocity was found to be one of the main influence quantities for Rockwell and Vickers scales, therefore its effect was evaluated in a previous work that indicated an effect much higher than expected. In that work some warning was given, because the analysis was based on the results obtained on a single Hardness Standard Machine, moreover based on a simple experimental plan that did not guarantee any separation of the effects of time and velocities. In the present work these drawbacks are overcome. The analysis is based on an experimental plan that takes into account the load increasing time, the velocity of the initial part of indentation and the velocity of the last part of indentation, that is for the Rockwell and the Vickers method the most important influence factor. Moreover, following the resolution adopted within the recent ISO TC 164/SC3 meeting during which Martens Hardness was extended to cover from nano to macro ranges, experiments are performed on each of these ranges and with different machines, delivering in that way more significant results.
Keywords:
Martens Hardness, Hardness Measurement, Uncertainty in Hardness Measurement, Hardness Standard Machine, Hardness Standardisation
Download:
IMEKO-TC5-2002-024.pdf
DOI:
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Event details
IMEKO TC:
TC5
Event name:
Joint International Conference on Force, Mass, Torque, Hardness and Civil Engineering Metrology in the age of globalization
Title:
8th HARDMEKO Conference on Hardness Measurement (together with 18th TC3 Conference on Force, Mass and Torque and 1st TC20 Conference on Civil Engineering Metrology)
Place:
Celle, GERMANY
Time:
24 September 2002 - 26 September 2002