ABSOLUTE VOLUME MEASRUMENET OF SILICON SPHERES AT NMIJ

Naoki Kuramoto, Kenichi Fujii
Abstract:
The method and devices for absolute volume measurements of 1 kg silicon spheres are described. An interferometer equipped with a direct optical frequency tuning system is used to measure the sphere volume, in which the optical frequency of a diode laser can be tuned continuously over a frequency range of 19 GHz. Accurate frequency changes in the laser produced by this system are used to measure the sphere diameters by phase-shifting interferometry. A total of seventy diameters, which are distributed near-uniformly over the surface of the sphere, are measured in vacuum. The volume of the sphere is determined by fitting the diameters to a series of spherical harmonics. The mass of the sphere is compared with that of the national prototype of the kilogram through a secondary 1 kg standard. The relative combined standard uncertainty in the density determined by direct measurements of the mass and volume is presently estimated to be 7.3ยท10-8. Recent results on the volume determination for three 1 kg silicon spheres are shown.
Keywords:
volume standard, density standard, silicon sphere, Avogadro constant
Download:
PWC-2006-TC3-032u.pdf
DOI:
-
Event details
Event name:
XVIII IMEKO World Congress
Title:

Metrology for a Sustainable Development

Place:
Rio de Janeiro, BRAZIL
Time:
17 September 2006 - 22 September 2006