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Francisco Javier Hernández Castro, Andrej Svete, Jože Kutin
METHOD FOR CORRECTION OF THE SYSTEMATIC ERRORS IN DETECTED SHOCK WAVE PASSAGE TIMES IN THE SHOCK TUBE

The most important uncertainty component of the pressure step signal determined at the end-wall of the shock tube is associated with the uncertainties of the shock wave velocity and the arrival time of the shock front. Both are determined using a time-of-flight method and are therefore greatly affected by the errors in the detected times of the shock wave passages over the side-wall pressure sensors installed along the shock tube. This paper introduces a method for an automated correction of the systematic errors due to non-ideal dynamic response of the side-wall pressure sensors.

C. Forssén, I. Silander, J. Zakrisson, E. Amer, D. Szabo, T. Bock, A. Kussicke, T. Rubin, D. Mari, S. Pasqualin, Z. Silvestri, D. Bentouati, O. Axner, M. Zelan
CIRCULAR COMPARISON OF CONVENTIONAL PRESSURE STANDARDS USING A TRANSPORTABLE OPTICAL REFRACTOMETER: PREPARATION AND TRANSPORTATION

Using a transportable Fabry-Pérot cavity refractometer, a circular comparison of existing primary standards at several national metrology institutes is currently underway. This paper provides information about the refractometer, the preparation for the comparison, and the transportation procedure.

D. Pantić, M. Burger, Z. Nikolić, I. Panić
PERFORMANCE OF ADAPTIVE MONTE CARLO PROCEDURES USING DIFFERENTIAL PRESSURE MEASUREMENT MODEL

Adaptive Monte Carlo procedure given in Supplement 1 to the “Guide to the expression of uncertainty in measurement” (GUM S1) and a modified GUM S1 procedure were applied to reach a prescribed numerical accuracy of the Monte Carlo results for a chosen confidence level. We assess the performance of the adaptive procedures by employing the measurement model that defines differential pressure generated by a pair of pressure balances. A large number of premature calculation terminations when applying the GUM S1 adaptive procedure leads to a low success rate. Applying the modified GUM S1 shows a reduction in premature termination and improves the success rate.

T. Rubin, I. Silander, J. Zakrisson, M. Hao, C. Forssén, P. Asbahr, M. Bernien, A. Kussicke, K. Liu, M. Zelan, O. Axner
THERMODYNAMIC EFFECTS IN A GAS MODULATED INVAR-BASED DUAL FABRY-PÉROT CAVITY REFRACTOMETER ADDRESSING 100 KPA OF NITROGEN

An Invar-based dual Fabry-Pérot cavity refractometer used for assessments of pressure by the gas modulation refractometry (GAMOR) methodology has been scrutinized with respect to the influence of thermodynamic effects (pV-work) that originates from the gas exchange process when 100 kPa of nitrogen is addressed. It is shown that the actual temperature variation of the cavity spacer solely is a fraction of the previously assessed upper limits (0.5 mK/100 kPa), limited to sub-parts-per-million (ppm) levels. This finding additionally supports the conclusion that the thermodynamic effects will not be a limiting factor when the system is used for assessments of pressure.

Z. Krajíček, D. Pražák, R. Páviš, M. Vičar, V. Sedlák, J. Tesař
EXPERIENCE WITH A NEW 1 GPa STANDARD OF THE CMI

The expansion of the high technology leads to the increasing demands for the calibration services in the extremal pressure ranges, both vacuum and high gauge pressure in liquid medium. The presentation will deal with the second one, focusing on the solution chosen by the Czech Metrology Institute (CMI) to improve its services in the range of gauge pressure from 0.5 GPa to 1 GPa. A new high-pressure standard will be described, and its first evaluation outlined.

T. Rubin, I. Silander, C. Forssén, J. Zakrisson, E. Amer, D. Szabo, T. Bock, A. Kussicke, C. Günz, D. Mari, R. M. Gavioso, M. Pisani, D. Madonna Ripa, Z. Silvestri, P. Gambette, D. Bentouati, G. Garberoglio, M. Lesiuk, M. Przybytek, B. Jeziorski, J. Setina, M. Zelan, O. Axner
‘QUANTUM-BASED REALIZATIONS OF THE PASCAL’: STATUS AND PROGRESS OF THE EMPIR-PROJECT: QUANTUMPASCAL

The QuantumPascal (QP) project combines the capabilities of 12 European institutions to enable traceable pressure measurements utilizing quantum-based methods that evaluate the number density instead of force per area to target the wide pressure range between 1 Pa and 3 MPa. This article summarizes the goals and results since the project start in June 2019.

I. Matas, L. Grgec Bermanec, T. Veliki
DESIGN AND DEVLOPMENT OF MEMBRANE PRESSURE REGULATOR FOR CRYOGENIC APPLICATIONS

This paper investigates different possibilities of measurement and control of pressure in the cryostat filled with liquid nitrogen. Laboratory designed membrane pressure regulator for automatic control of pressure in the range from 0.9 to 1.3 bar gauge in the cryostat is presented. The performance of the special purpose regulator is evaluated through measurement of pressure deviations from set-point value and their effect on thermal conditions in the cryostat. Results are compared to values obtained using manual pressure regulator.

S. Ehlers
IN-SITU LIQUID DENSITY MEASUREMENT FOR LIQUID COLUMN MANOMETRY

At PTB, an interferometric liquid column manometer for the pressure measurement up to 2 kPa is under development. Its in-situ liquid density measurement is a new approach for those primary pressure standards and makes the use of low-density liquids – low in comparison with the density of mercury, a liquid often used in other standards – possible. Such liquids, here, vacuum oils, offer an excellent sensitivity in length changes against pressure. The liquid density measurement concept is presented, together with the uncertainty estimation.

M. Morales, S. Higuera
AN INTERACTIVE APPLICATION FOR COMPARISON OF FIT APPROACHES IN BALANCES PRESSURE CALIBRATION

The calibration of a pressure balance implies to determine the values of the zero-pressure effective area A0 and the pressure distortion coefficient λ that defines the piston-cylinder assembly effective area Api. In order to analyze this behavior, this work compares the method of ordinary least squares with the generalized least squares and weighted least squares to calculate the contributions to type A uncertainty, in particular the residual deviation. For this purpose, an interactive application has been built in R- Shiny, which allows for getting the results mentioned.

S. Moltó, M. A. Sáenz-Nuño, C. García-Izquierdo, E. Bernabeu
A PARAMETRIC METHODOLOGY FOR THE ASSIGMENT OF PRESSURE VALUES VERSUS REFRACTIVE MEASUREMENT

The 18SIB04 QuantumPascal EMPIR project aims to achieve quantum-based pressure standards. One of the most promising ways of achieving this goal is the use of a Fabry-Perot interferometer for measuring the refractivity of the involved gas.
The refractivity and gas pressure are connected by the Claussius-Mossotti and Lorenz-Lorentz formal relations. However, these relations are based on “ideal assumptions”. The main scope of this research is how to solve this problem minimizing the use of the refractivity virial expansion by a parameter modifying the Lorenz-Lorentz relation. This methodology increases the physical quantum knowledge of the involved gases and develops a new procedure for determining the gas pressure from refractivity measurements.

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