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D. V. Silva, M. J. Sampaio, C. Milagres, V. Alves, F. Ferreira
Flow4Link - The flow in the hand

Due to greater awareness of the rationalization of water resources, Águas do Norte SA has a need to implement new methodologies to control water losses in order to improve the efficiency of their systems.
The Instrumentation&Automation team has developed some procedures, whose objective is to characterize the performance of the various flow meters, trying to reduce one of the components that define the apparent losses in water balance: measurement errors.
The present study has as scope the development of a work tool able to anticipate problems of measurement and equipment operation, in a park of flowmeters that totals about 950 flowmeters, some with about 20 years old and in different installation conditions than the initials. Safeguarding a minimum measurement chain uncertainties, several methods for information acquisition and identification of the flowmeters operating point and associated error were tested. For the calculation of the water balance, the improvement in the flow measurement will allow to quantify and possibly reduce a part of the apparent losses related to the measurement, which can be done in several ways: by replacing flowmeters with other more appropriate ones (reduction of diameter or measurement technology) or the change in operating way of some infrastructures.
The conclusions reached, highlighting the initial stage of the project, suggest that a part of the existing flow meters operate in operating ranges that are not the most adequate, taking into account the metrological characteristics of the meters, causing reading errors that contribute to the increase of apparent losses.

Jia Ren, Jiqin Duan, Yang Dong
Application and Uncertainty Analysis of a New Balance used in Natural Gas Primary Standard up to 60bar

A new 3-ton electromagnetic balance system was designed and built up for a high level mass-time primary standard of natural gas up to 60bar in CVB. The system is composed of a 3-ton electromagnetic balance, two tanks with thermal isolation, two platforms, two roller guide rails and two big weights which are used for special test. To achieve a lower uncertainty and the security application in natural gas measurement, several special methods were used in the system. Firstly, the tanks and platforms can be moved together steadily on the roller guide rail to be connected with pipeline system or to be weighted by the balance which also reduces the pipeline length between tanks and pipeline system. Secondly, the substitute weighing method is used for high accurate weighting. Finally, the whole system is located in a thermal isolated room with temperature and humidity controlling. Technical details, performance tests, uncertainty analysis and the future improvement ideas of the balance system are presented in the paper. The uncertainty analysis shows that the mass measurement uncertainty of gas can achieve less than 1.0g and the relative standard uncertainty of natural gas mass measurement can achieve less than 0.02%.

N. Takegawa, M. Ishibashi, T. Morioka
Effects of step in CFVN on Premature Unchoking Phenomena

CFVNs (Critical Flow Venturi Nozzles) are widely used as transfer standards and can realize the accurate measurement of the flow rate. However, previous research has reported that the pressure recovery effect of the diffuser deceases significantly in some CFVNs, and it has been called PUP (Premature Unchoking Phenomenon). In this study, we conducted experiments and investigated the CBPR (Critical Back Pressure Ratio) of the CFVNs. Additionally, in order to solve the PUP, we focused on the step in the diffuser and verified the its effect. As a result, although a backward facing step (causing increase of diameter) at the throat is effective for improving the CBPR at the Reynolds number of about 44000, it does not provide the improvement when the Reynolds number decreases to 11000. A forward facing step (causing decrease of diameter) in the diffuser delivers the desired pressure recovery even in the low Reynolds number of about 5000, and the CBPR can be improved. Therefore, the forward facing step in the diffuser is suggested to be a new countermeasure against the PUP in the low Reynolds number.

G. Vindišar, D. Škrbić, B. Simšič
Fuel dispensers in Slovenia - Between compliance and fairness

High level of public and legal interest concerning fuel dispensers’ measurements accuracy is always present. Surveillance of dispensers prior to 2013 reported undesired high error values. To limit possibilities of systematic favoring of single parties Slovenian national regulative was adapted. In year 2013 value of maximum permissible error at periodic verifications for higher flow rates of fuel dispensers was reduced. After one verification period passed Surveillance service of Metrology Institute of the Republic of Slovenia (MIRS) performed a surveillance of fuel dispensers seeking feedback information on implementation of modified requirements.
On over 150 petrol stations over 300 nozzles serving four different fuel types were controlled at two different fuel flow rates. More than 600 evaluated control results showed among others, that the average measured error at maximum flow rate Qmax amounted up to + 0,23 %, depending of the fuel type. Almost all measured errors were in line with the metrological requirements, 76 % of which however appeared to be in favor of the petrol station owner. Average deliveries at Qmax were less favorable to an end customer than deliveries at Qmin.
After another verification period surveillance was performed again. Average measured errors showed further reduction. Measurements also improved their symmetry.
Compliance of measuring instruments is not hindered by adapted regulative, while level of measurement fairness is apparently elevated.

Chao Yuan, Georgios Dimitrakis, Buddhika Hewakandamby
Measurement of water volume fraction in oil-water upward flow by using microwave cylindrical resonant cavity

A microwave resonant cavity was used for the determination of water volume fraction in oil-water upward flow, the frequency shift and changes in the quality factor of the cavity resonator were the vital parameters. During the experiments, the flow rates of silicon oil were 75, 100 and 125 L/min and the water volume fraction ranged from 0 to 20.1%. The relative error between the predicted and measured water volume fraction of oil-water upward flow ranged from -3.9% to 4.32% and -2.58% to 4.44% for the TM010 and TM110 modes.

Shinichi Nakao, Hiroshi Asano, Takeshi Yakuwa
Problems to note when using the nozzle to nozzle test method

The strange behaviors of the discharge coefficient of the critical nozzle were found when gradually changing the back pressure ratio (Pd/Pu) from the almost zero to the critical back pressure ratio in the nozzle to nozzle test method. When the test gas is Helium, the change amount of the discharge coefficients at these strange behaviors is quite large and seems significantly to influence to flow measurements. The causes of the strange behaviors are different in the ranges of Pd/Pu<0.1 and of Pd/Pu>0.1, and in either case are considered to be due to the measurement principle of the nozzle to nozzle test method that the mass flow rate through the system is constant. Under the condition that the mass flow rate is constant, the discharge coefficient of the critical nozzle on the downstream side in the nozzle to nozzle test method must definitely change in inverse proportion to its upstream pressure change. The flow models are suggested to explain the reason why the upstream pressure changes when changing the back pressure ratio. The more important point of the present results is that the equivalence of the discharge coefficient determined by the general calibration methods and by the nozzle to nozzle test method may be not always hold.

W. Maru, S. Lakshmanan, N. Singh, A. Thomas
Oil-Water Flow Measurement for Custody Transfer Applications

In the Oil & Gas industry, the ownership or custody transfer (CT) of crude oil is measured using Flow Metering and Sampling. Flow Metering quantifies the total amount fluid while Sampling quantifies the fluid composition – for example, the water fraction and other compounds thereby correcting the Flow Metering for its Oil-Cut. Any small inaccuracies in sampling may result in the sale or purchase of expensive water – resulting in significant financial exposure, incorrect government taxations and consequently affecting our weekly shopping too. Worse still, the absence of periodic sampling and failure to detect some undesirable compounds such as (inorganic and organic) chlorides could be catastrophic – not only economically but also politically. Therefore, the central tenet in Sampling is the creation of homogeneous mixture in the pipeline so that accurate representative samples could be extracted. However, achieving a homogeneous mixture of oil and water - two fluids that don’t like to mix, is challenging. To that end, following current industry standards, OGM has developed the SmartMix® Sampling System and tested it using two flow loops of different sizes, the SMPFL and LMPFL. For prototype development at the University of Cambridge, the SMPFL together with magnetic resonance imaging (MRI) is used to characterise the mixing profile. For industrial scale testing, the LMPFL together with Multiport Profile Proving (MPP) device is used to validate the performance and integrity of the technology. The test results achieved better than 97% mixing efficiency, significantly exceeding the 90% requirement stipulated by the current industry standards.

Ying-Chun Lin, Win-Ti Lin, Chun-Lin Chiang,
Establishment and Verification of Mercury-Sealed Piston Prover for Primary Standard

This paper presents the establishment and verification of a mercury-sealed piston prover, which is commonly used for low pressure gas flow calibration. The calibration gases could be dry air, nitrogen, argon, helium, oxygen and carbon dioxide. The flow capacity of the new system covers from 0.002 L/min to 40 L/min at 23 °C and 101.325 kPa, and some overlapped flows are between various columns. The relative expanded uncertainty of mass flow measurement is less than 0.08 % at 95 % confidence level.
We were also successfully altering the temperature sensor construction, temperature sensor placement, data logger system to real-time monitor the temperature difference of the entering gas. The data showed that the temperature difference between the entering gas and column could approximate in the calibration period.
The newly piston prover measurement result between different column was less than 0.01 %. A comparison between new-constructed and original CMC submitted piston prover that both are in CMS was conducted, and the En value was less than 0.4. The results indicate that the measurement capabilities of each column of newly piston prover were identical with expectation.

E. Batista, A. Furtado, J. Pereira, M. Ferreira, H. Bissig, E. Graham, A. Niemann, A. Timmerman, J. Alves e Sousa
New EMPIR project – Metrology for Drug Delivery

This document presents the scientific and technical objectives, state of the art and expected progress beyond it, and most importantly the expected impact on metrology, science, standards, and society of the new joint research project - MeDD II, Metrology for drug delivery (follow up of project MeDD I). It was selected for funding through the EURAMET EMPIR program of the European Commission and the participating countries. The project starts in June 2019 and will last for three years. It involves 15 partners from National and Designated Metrology Institutes, companies, and academia. The main objective is to enable traceable measurements of volume, flow and pressure of existing drug delivery devices (like, infusion pumps and analysers) and inline sensors that work at flow rates lower than 100 nL/min, in order to prevent inaccurate measurement results. This project will also investigate fast changing flow rates, liquid mixing behaviour and occlusion phenomena in multi-infusion systems with the purpose of improving dosing accuracy in each infusion line.

G. Kok, D. van Putten, L. Zakharov
Results from an intercomparison between multiphase flow test facilities

Multiphase flow meters are measurement instruments that simultaneously measure the flow rates of oil, natural gas and water flowing through a pipe line. Their traceability and the comparability of test results stemming from different multiphase test facilities is much less well established than that of single phase flow meters and single phase calibration facilities. In the (first) EMRP MultiFlowMet project an intercomparison for multiphase test facilities was organised to investigate the comparability of multiphase flow test facilities. Three facilities participated: NEL, DNV GL and OneSubsea-Schlumberger (OSS). VSL acted as independent partner auditing the uncertainty budgets, witnessing the tests and analysing the data. The outcome of this analysis was pairwise consistencies in the order of 80 %, taking into account the claimed uncertainties of the test facilities and the estimated meter reproducibility. This value was also found for the comparison with OSS, where a different inlet geometry was used. Open access to data and more extensive testing could provide means to get a better understanding of the reasons behind the inconsistency of a small part of the points.

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