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Sang-Woo Kang, Ju-Young Yun, Jin-Tae Kim, Yong-Hyun Shin, Jong-Yeon Lim
REAL TIME EVALUATION OF VACUUM PROCESS FOR THIN FILM ALUMINUM DEPOSITION

The chemical species in gas phase and on the surface of aluminum precursor (boro-hydride trimethylamine (ABHTMA)) for aluminum deposition process with the vacuum level and the hot wall temperature were studied using two kinds of Fourier transform infrared (FT-IR) spectroscopes which was installed at the end of the chamber. The absorbance of Al-H, B-H, C-H and C-N stretching features of the chemical species in the gas phase and on the surface was sensitive to the variation of analysis conditions. From those results, the temperature dependence of the film composition and quality could be explained.

Han Wook Song, Soo Young Kim, In Mook Choi, Chang Bog Kim, Kyung Don Yang
FABRICATION AND EVALUATION OF A PRESSURE SENSOR FOR THE MEASUREMENT OF A DYNAMIC PRESSURE

The sensor for the measurements of a dynamic pressure was developed and evaluated. Quartz was adopted as a piezoelectric medium to transmit a pressure signal and a sensor was made from SM45C. Positive going step method was used to evaluate sensors. The developed sensor showed a linear response property till 300 MPa and a repeatability error below ± 3 %. The sensor showed a similar sensitivity and a poor repeatability compared to commercial pressures. But we expected our sensor had a competitiveness considering the production cost and the repeatability could be improved if the packaging technique might be improved.

Yasin Durgut
THE EVALUATION OF INTERLABORATORY COMPARISON IN HYDRAULIC PRESSURE REGION

Inter laboratory studies serve several needs and aspects of the quality management of measuring measurements. Inter laboratory comparisons are important for the laboratories to assess their own measurement capability. In this paper, results of the inter laboratory comparisons in pressure metrology at two measurement scopes are presented. The artefacts used for these inter laboratory measurement scopes are analogue and digital manometers in hydraulic pressure and 250 bar and 700 bar ranges. Also 12 different laboratories joined as participant and these laboratories made more than 12 measurements in two different measurement scopes.

Kenta Arai, Hajime Yoshida, Hitoshi Akimichi, Tokihiko Kobata
VOLUME CHANGE MEASUREMENT OF DIAPHRAGM DEFORMATION IN DIFFERENTIAL TYPE CAPACITANCE DIAPHRAGM GAUGE

A deformation of a diaphragm inside a differential type capacitance diaphragm gauge is investigated as a function of the differential pressure applied to the gauge. Below its full scale of 133 Pa, the volume change of the gauge is proportional to the applied pressure as predicted by the elastic theory. The volume change rate of the gauge is calculated to be 0.00012 ml/Pa at a line pressure of atmosphere pressure of about 100 kPa. When the pressure is more than its full scale, the response of the diaphragm volume change is linear to the applied pressure until 500 Pa. The response is changed to one-third power of the applied differential pressure as predicted by the membrane theory above 500 Pa until 3000 Pa.

SamYong Woo, In-Mook Choi, Tae Heon Yang, HanWook Song
CHARACTERISATION OF 10 Pa VACUUM GAUGE USING PRESSURE BALANCE

This paper presents an extended usage of gas pressure balances for measurements of pressure down to below 10 Pa. This pressure range is too low to measure by using commercial pressure balances. This is because their inability to operate at pressures below a limit determined by the mass of floating elements. Using a variable bell-jar pressure method developed at KRISS, we can overcome this pressure limit. Additionally, we investigated the lowest achievable pressure limit using commercial 133-Pa CDG (Capacitance Diaphragm Gauge).

M. Jeráb, T. Gronych, L. Peksa, F. Stanek, Z. Krajícek, D. Pražák, M. Vicar, J. Tesar
MULTI-OPENING ORIFICE - A TOOL FOR PRIMARY METROLOGY OF VACUUM AND SMALL GAS THROUGHPUTS

Multi-opening orifice is a device for gas flow and related vacuum quantities primary measurement. It keeps molecular flow regime and thus possibility to calculate the conductance very accurately from geometrical dimensions up to relatively high pressure. Moreover, the value of the total conductance could be sufficiently high to achieve reasonable parameters of the used vacuum system. Suitable shape of a multi-opening orifice duct and principles of multiopening orifice design are discussed. An example of the multi-opening orifice manufactured with grinding is given. Limits and requirements for further development are drafted.

H. Yoshida, E. Komatsu, K. Arai, M. Kojima, H. Akimichi, T. Kobata
CALIBRATION OF CAPACITANCE DIAPHRAGM GAUGE WITH 1333 PA FULL SCALE BY DIRECT COMPARISON TO RESONANT SILICON GAUGE AND STATIC EXPANSION SYSTEM

Two capacitance diaphragm gauges (CDGs) with 1333 Pa full scale were calibrated by three different methods; direct comparison to a resonant silicon gauge calibrated by a pressure balance, direct comparison to a CDG with 133 Pa full scale calibrated by a static expansion method, and the static expansion method. The calibration results by the three calibration results show in good agreement within their claimed uncertainties. It is demonstrated that calibrated pressure points by the pressure balance and the static expansion system are linearly interpolated by considering the calibration uncertainty of the CDGs appropriately.

H. Kajikawa, T. Kobata
METHODS FOR ENHANCING REPRODUCIBILITY OF CALIBRATION RESULTS FOR HYDRAULIC PRESSURE TRANSDUCERS

The effects of the calibration procedure on the results are investigated for quartz Bourdon-type hydraulic pressure transducers. A fully-automated system that uses a pressure balance as the standard device has been developed for the calibrations at pressures from 10 MPa to 100 MPa. The effect of the interval between the calibration cycles and the effect of preliminary pressurization are quantitatively evaluated for two kinds of calibration cycles, stepwise and 0-A-0-type calibration cycles. For the stepwise cycle, the interval between the calibration cycles strongly affects the results in the pressure increasing process. The preliminary pressurization reduces the influence of the interval on the results. However, in turn, the waiting time between the preliminary pressurization and the main calibration cycle exerts a strong influence on the results. For the 0-A-0-type calibration cycle, the effect of the interval on the results is almost half of that for the stepwise cycle. Moreover, with preliminary pressurization, the calibration results are rarely affected by the interval. From the results, possible methods for obtaining reproducible calibration results are discussed.

Luiz Henrique Paraguassú de Oliveira, Jackson S. Oliveira, Paulo Roberto Guimarães Couto, Arthur M. Braga
ALTERNATIVE METHOD TO MEASURE PRESSURE USING OPTICAL FIBER

A number of different measurement principles are used in pressure measuring instruments. Some principles use fundamental methods and others can use some property of the material, like a mechanical deformation of a sensing element to determine a quantity. Following this possibly of measuring pressure through a physical property, it was created a new kind of pressure sensor that uses guided light in an optical fiber as measurement principle. This new technology has been used in pressure sensors mainly for the petroleum industries by measuring the variations of the wavelength associated with pressure values. Compared with pressure sensors that use traditional technologies of measurement, optical sensors have shown a growing acceptance because they have a good behaviour in harsh and hostile work conditions. This paper describes a calibration system established to evaluate the metrological features of this pressure optical sensors showing up the calibrations results.

A. Jeerasak Pitakarnnop
RAREFIED GAS FLOW IN PRESSURE AND VACUUM MEASUREMENTS

Flows of a gas through piston-cylinder gap of a gas-operated pressure balance and in general vacuum system have one similar aspect, i.e., the gas is rarefied due to small passage and low pressure, respectively. The flows in both systems could characterize in either slip flow regime or transition regime. Therefore, fundamental researches of flow in these regimes are useful for both pressure and vacuum metrology, especially for the gas-operated pressure balance where continuum viscous flow model is widely used for determining an effective area of pressure balance. The consideration of gas flow using suitable assumption would improve the accuracy of such calculation. Moreover, knowledge in rarefied gas flow contributes a predictability of gas behaviors in vacuum and low-flow leak detection system. This paper provides useful information of rarefied gas flow in both slip flow and transition regimes.

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