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Krzysztof Stepien, Stanislaw Adamczak
RESEARCH ON ACCURATE IN SITU MEASUREMENTS OF CYLINDRICITY

In many industries (for example, in paper, electric or ship industry), large and heavy cylindrical elements play very important role. Such workpieces should posses very good quality of form and dimensions. Sometimes, they may be deformed under certain operating conditions, e.g. due to a high temperature or great external or internal loads. Consequently, wear and damage of the working surfaces are observed. Therefore cylindricity deviations of such workpieces should be measured during their manufacturing and exploitation. However, some of the workpieces cannot be measured accurately by existing measuring instruments because they are too large or too heavy and therefore they cannot be placed on the measuring table of the instrument. This is why the industries manufacturing or applying cylinders expect that measurements of cylindricity profiles will be made directly on the machine tool or in the work area. In the paper methods allowing such measurements are investigated. The methods are divided into two main groups: multisensor and V-block methods. Most important advantages and disadvantages of both groups of methods allowing accurate in situ cylindricity measurements are given as conclusions.

Dariusz Janecki, Krzysztof Stepien, Stanislaw Adamczak
CALCULATION OF REFERENCE SURFACE PARAMETERS FOR ELEMENTS WHOSE GENERATRIX IS A FRAGMENT OF A CIRCLE

Accurate measurement of irregularities of the geometrical surface structure requires mathematical definition of relevant reference surface, which is called according to the newest terminology, an associated surface. Such surface is the reference feature in relation to which appropriate surface parameters are calculated. When measuring cylindricity deviations, the least squares or minimum zone cylinders have been mostly used as associated features. However, an ideal cylinder cannot be employed as an associated feature when measured elements are not nominally cylindrical but for example barrel- or saddle-shaped. The paper presents mathematical model of calculation of the associated feature for elements whose generatrix is the fragment of a circle and results of the experimental verification of developed concept.

Elena Amico di Meane, Davide Baroncini, Stefano Crispu, Gian Carlo Piras, Michela Sega
INTEGRATE APPROACH TO THE CALIBRATION OF NITROGEN OXIDES ANALYSERS AND TO THE EVALUATION OF THEIR MEASUREMENT UNCERTAINTY

The present work describes the approach to evaluate in a metrological correct and exhaustive way the contribution of the several sources to the uncertainty related to the calibration of nitrogen oxides (NOX) analysers, focusing in particular on non dispersive infrared (NDIR) analysers. In order to minimize the contribution due to the uncertainty on the composition of the calibration standards, gas mixtures of NOX prepared with the gravimetric method are used. The performances of two different techniques, namely NDIR and chemiluminescence, are compared by analysing primary reference gas mixtures prepared at the Istituto Nazionale di Ricerca Metrologica (INRIM), having concentrations within 100 mmol·mol-1 of NOX.

Elsa Batista, Nelson Almeida, Eduarda Filipe, João Alves e Sousa
COMPARISON OF TWO DIFERENT APPROACHES IN THE UNCERTAINTY CALCULATION OF GRAVIMETRIC VOLUME CALIBRATION

The uncertainty calculation in the calibration of volumetric instruments is normally performed with the classical approach of the “mainstream GUM”. In order to validate the obtained results, since there is a degree of non linearity involved in handling the corresponding expression of volume, a Monte Carlo method was used as a second approach for calculation of that measurement uncertainty. The results of this comparison and corresponding conclusions are presented.

Jun Liu, Ting Huang, Wei Zhang, Yang Liu
DEVELOPMENT OF A CERTIFIED REFERENCE MATERIAL FOR NICOTINAMIDE IN INFANT FORMULA

Nicotinamide, one kind of Vitamin B, plays an important role for humans. To ensure quality control of nicotinamide in infant formula, a Certified Reference Material for nicotinamide in infant formula is being prepared in China for the first time. Studying on the procedure of sample preparation and HPLC analysis with different detectors like UV and MS, HPLC-UV and HPLC-IDMS are selected as the value assignment methods. And HPLC-IDMS method was validated in the international comparison CCQM-P78 and CCQM-K62. Homogeneity and stability are discussed in this paper as well.

Monludee Ranusawud, Ketsaya Vacharanukul, Anusorn Tonmueanwai
TRACEABILITY OF 633 nm LASER CALIBRATION AT NIMT

The National Institute of Metrology (Thailand), NIMT, maintains the standard of length in accordance with the definition of the meter through a 633 nm iodine stabilized He-Ne laser. Its accuracy is transferred to stabilized and non-stabilized lasers regarding to beat-frequency method and direct measurement using a wavelength meter, respectively. The traceability in wavelength measurement at the NIMT is discussed here. The iodine stabilized He-Ne laser is self-calibrated using the master and slave beat frequency system. NIMT participated in APMP.L-K11 intercomparison and the results are presented. The standard uncertainty is 2.5 × 10-11.

Yon-Kyu Park, Rolf Kumme, Dirk Röske, Dae-Im Kang
EVALUATION OF MULTI-COMPONENT FORCE TRANSDUCERS HAVING COLUMN TYPE SENSING ELEMENT

We describe the dynamic evaluation of two multi-component force-moment transducers having column-type sensing element. Among them, one has a solid cylindrical sensing element and the other has a hollow cylindrical shape. They were calibrated statically with a force-moment calibration machine in the Physikalisch-Technische Bundesanstalt (PTB), Germany. We evaluated the dynamic characteristics of the force-moment transducers by using a shaker system and a multi-channel dynamic analyser system. We have examined and presented basic dynamic characteristics of the force transducers. In this paper, we will describe the dynamic characteristics of the force transducers in detail.

David Martin, Derek G. Chetwynd
ANGLE CALIBRATION OF ROBOTIC TOTAL STATIONS AND LASER TRACKERS

This paper presents the recent development of two angle standards used for the calibration of high precision spherical measurement systems. These systems are a family of instruments comprising robotic total stations, and laser trackers. It discusses the Horizontal Circle Comparator and the Vertical Circle Comparator, the way they function and are used, their uncertainty, and results of instrument calibrations.

Gaoliang Dai, Herrmann Konrad, Febo Menelao
PROGRESS IN THE CHARACTERIZATION OF THE GEOMETRY OF ROCKWELL DIAMOND INDENTERS

In this paper two methods for an improved characterization of the geometry of Rockwell diamond indenters are investigated: The establishment of a group standard of indenters and the derivation of an area function with a nano measuring machine. A group standard of indenters yields better statistical results than the calibration using only one indenter. Further, a group standard of indenters guarantees a higher stability of the Rockwell hardness scales in the case that an indenter is damaged and must be replaced by a new one. The second approach is based on the correction of the hardness test values using the indenter's area function determined by a high accuracy nano measuring machine. The investigation has proven that the range of the hardness deviations of a group of three Rockwell indenters amounting to ca. 0.4 HRC by the application of an area function with corrected hardness values can be further reduced to < 0.2 HRC for the lower hardnesses and to < 0.3 HRC for the higher hardnesses. The mean deviation of HRC values measured by this group of Rockwell indenters has been reduced from 0.11 HRC to 0.06 HRC by using the proposed correction method. In future correction methods for Rockwell diamond indenters usable for all standardized Rockwell hardness scales should be derived.

Carlos A. Fernandes, Jorge R. Costa
PERMITTIVITY MEASUREMENT AND ANISOTROPY EVALUATION OF DIELECTRIC MATERIALS AT MILLIMETER-WAVES

This paper describes the design and use of an open Fabry-Perot resonator to evaluate the degree of anisotropy of dielectric material samples at millimeter-waves. The proposed implementation not only allows identifying the orientation of the dielectric principal axes but also determining the complex permittivity values along these axes.

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